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For each serum sample, two experiments were completed at 310 K: a 1 H one-dimensional experiment with solvent presaturation (32 scans, 98 k data points, 30 ppm spectral width) and a Carr Purcell Meibo-Gill (CPMG) spin-echo experiment (32 scans, 74 k data points, 20 ppm spectral width)

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The `incretin effect was coined by Creuzfeld and Ebert in 1985 to designate this phenomenon [7]